Y Please enable Javascript in your browser. This page requires the MDL Chemscape Chime Plugin. By using this website, you agree to the use of cookies in accordance with our guidelines. 1 U Emergency Planning and Community Right-to-Know Act (42 U.S.C. R m/z Click and drag to zoom, double click to reset zoom Hover over end of line for value. I Specializing in ready to use metabolomics kits. Leave A Message All mass spectra in this site (plus many more) are available from the NIST/EPA/NIH Mass Spectral Library. L Benzyl chloride is prepared industrially by the gas-phase photochemical reaction of toluene with chlorine:C6H5CH3 + Cl2 → C6H5CH2Cl + HClIn this way, approximately 100,000 tonnes are produced annually. M Chemical Encyclopedia Partners CAS Number Search, Compound Synonyms benzoic acid. Q Your message has been sent. 1H NMR spectroscopy at 400 MHz has been applied to the analysis of whole bile samples produced by the isolated perfused rat liver. iodobenzene. Z X N 4 Chemical Encyclopedia benzyl chloride (NMR Spectrum) This page requires the MDL Chemscape Chime Plugin. 1 Day, Benzyl-d7 chloride 99+ atom % D Material Safety Data Sheet, Chloromethylbenzene; alpha-Chlorotoluene; Chlorophenylmethane; Benzyl chloride. P 1985;(16):41-4. 1,2-dichloroethane. 7 protons This page requires the MDL Chemscape Chime Plugin. Suppliers D benzyl chloride 1d (1.0 equiv, 1.0 mmol, 134 μL) and tert-butyl isocyanide (1.5 equiv, 1.5 mmol, 170 μL) were added in turn by syringe. In contact with mucous membranes, hydrolysis produces hydrochloric acid. J Application Benzyl chloride can be used as: • A benzylating agent for the benzylation of benzene and other aromatic compounds. Tags:Benzoyl chloride(98-88-4) 1 H NMR Related Products. 1H NMR spectroscopy at 400 MHz has been applied to the analysis of whole bile samples produced by the isolated perfused rat liver. Benzyl chloride is a potentially toxic compound. C 7 M 9, Home Benzyl chloride is possibly neutral. I About Us W Disclaimer, Copyright © 2013-2020 MOLBASE All Rights Reserved ICP Shanghai 14014220, Lead Time: Privacy Policy 11002), and is subject to strict reporting requirements by facilities which produce, store, or use it in significant quantities. E 2-Chlorobenzoyl chloride(609-65-4)IR2 2-Chlorobenzoyl chloride(609-65-4) Raman 2-Chlorobenzoyl chloride(609-65-4) 13 CNMR 2-Chlorobenzoyl chloride(609-65-4) 1 HNMR 2-Chlorobenzoyl chloride(609-65-4)MS 2-Chlorobenzoyl chloride(609-65-4)IR1 Benzyl chloride(100-44-7)IR1 Benzyl chloride(100-44-7) 1 HNMR Benzyl chloride(100-44-7)Raman Benzyl … V Disclaimer, Copyright © 2013-2020 MOLBASE All Rights Reserved ICP Shanghai 14014220, Lead Time: E T O Contact Us T ChemicalBook ProvideBenzoyl chloride(98-88-4) 1H NMR,IR2,MS,IR3,IR1,1H NMR,Raman,ESR,13C NMR,Spectrum p-dinitrobenzene. 1-bromo-2-chloroethane. 2-chloropropane. Keywords: 1H NMR; 13C NMR; 2D NMR; Benzyl o–Vanillin. Using relatively simple NMR experiments biliary excretory products of cefoperazone and benzyl chloride were identified as cefoperazone itself and a benzyl-glutathione conjugate, respectively. benzyl chloride. L Terms & Conditions Leave A Message Please try again later, or contact Restek or your local Restek representative via phone. 1-bromo-2-chloroethane. benzyl chloride . 2 P benzyl chloride 100-44-7 MSDS report, benzyl chloride MSDS safety technical specifications search, benzyl chloride safety information specifications ect. 5 4 GC Mass Spectrum. 8 About Us Products iodobenzene. 8 Synonyms . It is preferable over benzyl bromide for the preparation of this reagent, since the reaction of the bromide with magnesium tends to form the Wurtz-coupling product 1,2-diphenylethane. benzyl chloride (NMR Spectrum) This page requires the MDL Chemscape Chime Plugin. D 3 toluene. toluene. ChemicalBook ProvideBenzyl chloride(100-44-7) 1H NMR,IR2,MS,IR3,IR1,1H NMR,Raman,ESR,13C NMR,Spectrum Business Cooperation Molecular Weight: 126.5835: Formula: C 7 H 7 Cl: Melting Point −39 °C: Boiling Point: 179 °C: Density: 1.100 g/cm 3: Data above sourced from ChemSpider and Wikipedia. acetophenone. Compound Structure and Properties. S Benzyl chloride, also known as alpha-chlortoluol or a-chlorotoluene, belongs to the class of organic compounds known as benzyl chlorides. Other methods of production exist, such as the Blanc chloromethylation of benzene. Reset display : Structure: Proton Equivalence : … 6 Restek Corporation, U.S., 110 Benner Circle, Bellefonte, PA 16823Copyright © 2020 Restek Corporation. [, Akashi M, Tokiyoshi T, Miyauchi N, Mosbach K: Affinity chromatography of nucleosides and nucleic acid base derivatives with nucleic acid bases or nitrobenzeneboronic acid substituted silicas. G Products Structure Benzyl chloride (BzCl) is an organochlorine compound, which is widely used in organic synthesis for the preparation of useful chemical building blocks. G H vinyl acetate. InChI=1S/C7H7Cl/c8-6-7-4-2-1-3-5-7/h1-5H,6H2, The Metabolomics Innovation Centre (TMIC). 1,2-dichloroethane. +86-400-6021-666 service@molbase.com The reaction mixture was stirred at 100 °C oil bath until complete acetaldehyde dimethyl acetal. C This page requires the MDL Chemscape Chime Plugin. 2-chloropropane. benzyl chloride. : A acetophenone. J vinyl acetate. R Quantitative metabolomics services for biomarker discovery and validation. 1978;26(3):97. Chemical Product X Z It is classified as an extremely hazardous substance in the United States as defined in Section 302 of the U.S. Please see the following for information about the library and its accompanying search program. 3 Day, Lead Time: W belongs to the class of organic compounds known as benzyl chlorides. CAS Number Search, Compound Synonyms acetaldehyde dimethyl acetal. benzyl chloride 100-44-7 NMR spectrum, benzyl chloride H-NMR spectral analysis, benzyl chloride C-NMR spectral analysis ect. S We present an in-depth study of the acetylation of benzyl alcohol in the presence of N,N-diisopropylethylamine (DIPEA) by nuclear magnetic resonance (NMR) monitoring of the reaction from 1.5 s to several minutes. Phenylacetic acid, a precursor to pharmaceuticals, is produced from benzyl cyanide, which is generated by treatment of benzyl chloride with sodium cyanide. It is classified as an extremely hazardous substance in the United States as defined in Section 302 of the U.S. It is used for a variety of heteroatomic functional groups as well as carbon nucleophiles, so, this benzylation is used to protect hydroxyl group. Emergency Planning and Community Right-to-Know Act (42 U.S.C. Y 5 benzoic acid. 3 Suppliers Terms & Conditions Q 3 Day, Lead Time: 1 Day, More benzyl chloride NMR spectra of reference. K U [. Business Cooperation Derm Beruf Umwelt. We will be in touch shortly. B Your source for quantitative metabolomics technologies and bioinformatics. Benzyl chloride; Benzene, (chloromethyl)-; Toluene, α-chloro-; α-Chlorotoluene; ω-Chlorotoluene; (Chloromethyl)benzene; Chlorophenylmethane; C6H5CH2Cl; a-Chlorotoluene; α-Chlortoluol; Benzile(cloruro di); Benzylchlorid; Benzyle(chlorure de); Chlorure de benzyle; NCI-C06360; Benzile; Benzyle; Rcra waste number P028; Phenylmethyl chloride; a-Chlortoluol, Click and drag to zoom, double click to reset zoom, Drag and Drop Attachments Here (optional), TO-15 (HJ759) + PAMS on Rt-Alumina BOND/MAPD (by FID) and Rxi-624Sil MS (by MS) using Deans Switch, NJ Low Level TO-15 75 Component Mix on Rtx-VMS (60 m, 40 °C start), NJ Low Level TO-15 75 Component Mix on Rtx-VMS (30 m, 2.0 mL/min), TO-15 65 Component Mix on Rxi-5Sil MS (30 m), TO-15 65 Component Mix on Rtx-VMS (30 m, 1.2 mL/min), TO-15 65 Component Mix on Rtx-VMS (30 m, 2.0 mL/min), TO-15 65 Component Mix on Rxi-5Sil MS (30 m, 1.5 mL/min), TO-15 65 Component Mix on Rxi-5Sil MS (30 m, 2.0 mL/min), TO-15 65 Component Mix on Rxi-624Sil MS (30 m). B Privacy Policy Structure Sorry, your message could not be sent at this time. F 2 Benzyl chloride is a potentially toxic compound. anisole. Partners Benzyl chloride CAS # 100-44-7. Phenylacetic acid, a precursor to pharmaceuticals, is produced from benzyl cyanide, which is generated by treatment of benzyl chloride with sodium cyanide. Contact Us K For more information, see our privacy policy. H anisole. Using relatively simple NMR experiments biliary excretory products of cefoperazone and benzyl chloride were identified as cefoperazone itself and a benzyl-glutathione conjugate, respectively. Benzyl chloride is prepared industrially by the gas-phase photochemical reaction of toluene with chlorine: : A V We have adapted the NMR setup to be compatible to microreactor technology, scaling down the typical sample volume of commercial NMR probes (500 μL) to a microfluidic stripline … +86-400-6021-666; service@molbase.com ; Sign in; Register; About Us; Chinese; Search Batch Search. 7 Chemical Product These are organic compounds containing a benzene skeleton substituted with a chloromethyl group. 9, Home p-dinitrobenzene. These are organic compounds containing a benzene skeleton substituted with a chloromethyl group. All rights reserved. Nucleic Acids Symp Ser. 1 O This site requires that Javascript be enabled. N splash10-0006-9200000000-47bb06f55920c2d12977, splash10-0006-9300000000-c3afd89818a380776911, splash10-0006-9100000000-c16850c6c68fce3df5e9, Predicted GC-MS Spectrum - GC-MS (Non-derivatized) - 70eV, Positive, splash10-0006-9100000000-8ef8bfeb88ad3a17a4c2, Predicted LC-MS/MS Spectrum - 10V, Positive, splash10-004i-2900000000-79e607dd40bcd3c76d06, Predicted LC-MS/MS Spectrum - 20V, Positive, splash10-004i-5900000000-7b5d0e7df148f6543c41, Predicted LC-MS/MS Spectrum - 40V, Positive, splash10-0006-9000000000-72b99508ef9ad7785de5, Predicted LC-MS/MS Spectrum - 10V, Negative, splash10-004i-1900000000-1e23c9d141babbfed70e, Predicted LC-MS/MS Spectrum - 20V, Negative, splash10-004r-5900000000-04ead0ed95dd1c13e806, Predicted LC-MS/MS Spectrum - 40V, Negative, splash10-002r-9400000000-6ebfc4036fb58624c731, splash10-0006-9200000000-2a392f002d8b7024e9b6, Ippen H, Liebeskind H: [Contact eczema caused by 1,4-bis-chloromethylbenzene].